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As shown in Fig. ****, two homogeneous samples, each 3 mm in thickness, were cut out from high-speed cut samples cast from steels. The steel plates were first heated to 100°C, and then the temperature raised to the end of the zone 3 (100-200°C range) and then raised to the start of the zone 2 (200-600°C range). The heating was sustained until an area with a diameter of 3 mm underwent a maximum of 10 min in the 200-600°C range. The specimens were then sprayed with the flux and welded according to the 15-10 welding sequence and environmental conditions on a commercial SGC type 235 Ramming System, and then natural cooled over 2 hr. The heat treatment and welding procedures were applied so as to guarantee certain mechanical behaviors and stress-strain curves. SAE EN 2269-2004 - SGC welding at the base metal for domestic pipelines - was used for the welding of steels in the BM, HAZ and WB.

A nano-indentation test was applied on the HAZ at the crack tip to obtain the stress-strain curve. The nano-indentation experiment was conducted in accordance with ASTM E3120-03. In discussion with industry experts, a reduced-size model of the API 5L X52 steel plates was adopted and the ultimate tensile stress (UTS) and elastic modulus were determined to be about 70 MPa and 1.74 GPa, respectively. The reduced-size model was made automatically by using the nanoindentation size analysis software Nano indenter 6.0 (Copyright 2007, NetForce, Sweden), using an 80-mN load cell with a load repetition of 10 on the base metal. Using the reduced-size model, the hardness, Vickers hardness (HV) and UTS were calculated. The reduced-size hardness had a good correlation with an average indention, with a coefficient of determination R2 = 0.99.

The tensile stress-strain curve of the BM, HAZ and WB was obtained from the tensile tests. The curve for the BM was shown in Fig. ****. The points where the curves crossed included three yield stress points at about 54.

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